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Series 4540 600-1200 mL High Pressure Reactors
Series 4540 600-1200 mL High Pressure Reactors
4544 Floor Stand Reactor, 600 mL, Moveable Style
Vessel, with Heater Lowered and a 4843 Controller
Series 4540 600-1200 mL High Pressure Reactors
This series of stirred reactors has been designed for users who need higher operating pressures than the 2000 to 3000 psi offered by the General Purpose Reactor, but do not require the high operating temperatures provided by the Series 4570 High Pressure-High Temperature Reactors. These reactors offer working pressures to 5000 psi (345 bar) at temperatures to 350 °C.
(Shown at Left) Model 4546C Reactor, 1200 mL, Moveable Head Style, on a Moveable Cart.
These vessels have been designed with outside dimensions comparable to the Series 4520 and 4530 Reactors so that they can use the same support system, stirrer drive and heater as these popular general purpose models. This provides not only an attractively priced high pressure/moderate temperature system, but also reactors that can be interchanged with the 1 and 2 liter sizes. The thicker walls required for higher operating pressures reduce the volumes of these reactors to 600 and 1200 mL.
These reactors can be used in either the bench top or floor stand mountings. While the 1200 mL reactor is offered as a “bench top model”, it is too tall and too heavy to be handled comfortably on a standard height bench top. It is recommended that the floor stand support option should be selected unless the user has an “adjustable bench top” which will accommodate the overall height of the 1200mL systems.
Series 4540 Reactor Specifications
| Shading indicates specifications that change within models |
| Model Number | 4544 | 4545 | 4546 | 4547 |
| Sizes, mL | 600 | 600 | 1200 | 1200 |
| Max. Pressure | 5000 psi (345 bar) | |||
| Max. Temperature | ||||
| with FFKM 0-ring | NA | |||
| with PTFE Flat Gasket | 350 °C | |||
| Vessel Style | Movable | Fixed Head | Movable | Fixed Head |
| Reactor Mounting | Bench Top or Fixed Floor Stand, Moveable Floor Stand (Cart) Also Available | |||
| Closure (Cap Screws) | Split-Ring (8) | |||
| Valve Connections | 1/4" Male NPT | |||
| Magnetic Stirrer, Model No. | A1120HC* | |||
| Maximum Torque | 16 Inch-Pounds | |||
| Impeller(s), 6-Blade | 2 | |||
| Pressure Gage Size | 4.5 inches | |||
| Range | 0-7,500 psi (517 bar)* | |||
| Temperature Measurement | Thermowell | |||
| Cooling Coil | Included | |||
| Style | Single Loop | |||
| Bottom Drain Valve | A177VB | |||
| Heater Style | Calrod | |||
| Heater Power Watts | 1500 | 2000 | ||
| Stirrer Motor* | 1/8 hp variable speed | 1/4 hp variable speed | ||
| Electrical Supply | ||||
| Volts | 115 or 230 | |||
| Maximum Load | 16/8 amps | |||
| Vessel Dimensions | ||||
| Inside Diameter | 3.25 inches | |||
| Inside Depth,inches | 4.7 | 9.8 | ||
| Weight of Vessel, pounds | 51 | 57 | ||
| Reactor Dimensions | ||||
| Width, inches w/o Controller | 16.5 | 18 | ||
| Depth, inches | 23 | 23.5 | ||
| Height, inches | 33 | 75 | ||
| Weight, pounds w/Controller | 160 | 250 | ||
| Spare Parts Kit | 4549M | |||
Series 4540 Ordering Guide
A composite identification number to be used when ordering a reactor can be developed by combining individual symbols from the separate sections
Example A 600mL, T316SS, removable head reactor with magnetic drive, Flat Gasket, 115V explosion proof 1/4 hp motor, 3000 psi gage and programable controller with pressure display module would be listed as:
| No. 4544-T-SS-115-XP.25-3000-4843-PDM Model Gasket Material Voltage Motor No.4544 -T -SS -115 -XP.25 -etc.... A B C D E F
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